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A deep learning based automatic defect analysis framework for In-situ TEM ion irradiations

Videos captured using Transmission Electron Microscopy (TEM) can encode details regarding the morphological and temporal evolution of a material by taking snapshots of the microstructure sequentially. However, manual analysis of such video is …

Deconvoluting the Effect of Chromium and Aluminum on the Radiation Response of Wrought FeCrAl Alloys After Low-Dose Neutron Irradiation

FeCrAl alloys have been extensively investigated over the past decade as a candidate material for accident-tolerant fuel cladding in light water reactors. This work completes a first of its kind study where Al and Cr concentrations are varied …

Microstructures and mechanical properties of a modified 9Cr ferritic-martensitic steel in the as-built condition after additive manufacturing

A newly developed nano-structured high-Mn 9Cr ferritic-martensitic (FM) steel designed for additive manufacturing (Additive-manufactured Nanostructured Alloy, ANA) was fabricated via the direct energy deposition method. The as-printed ANA2 showed …

STEM Characterization of Dislocation Loops in Irradiated FCC Alloys

In this study, we demonstrate the methodology systematically developed for dislocation loop (perfect and faulted loops) imaging and analysis in irradiated face-centered-cubic (FCC) alloys using scanning transmission electron microscopy (STEM). …

Microstructural characterization of cold-worked 316 stainless steel flux thimble tubes irradiated up to 100 dpa in a commercial Pressurized Water Reactor

Two flux thimble tubes (FTTs) made of 15\% cold-worked 316 stainless steel (SS) were harvested from Ringhals Pressurized Water Reactor (PWR) Unit 2, with peak damages of 76 and 100 displacements per atom (dpa) after 29 and 34 years' service, …

Microstructure response of ferritic/martensitic steel HT9 after neutron irradiation: Effect of temperature

The ferritic/martensitic steel HT9 was irradiated in the BOR-60 reactor at 650, 690 and 730 K (377, 417 and 457 °C) to doses between ∼14.6–18.6 displacements per atom (dpa). Irradiated samples were comprehensively characterized using analytical …

High-Efficiency Three-Dimensional Visualization of Complex Microstructures via Multidimensional STEM Acquisition and Reconstruction

Complex material systems in which microstructure and microchemistry are nonuniformly dispersed require three-dimensional (3D) rendering(s) to provide an accurate determination of the physio-chemical nature of the system. Current scanning transmission …

Hydrothermal corrosion of 2nd generation FeCrAl alloys for accident tolerant fuel cladding

As part of an effort to develop advanced fuel cladding for use in light water reactors, several FeCrAl alloys have been developed at Oak Ridge National Laboratory. A second generation of these alloys bearing additional alloying elements over the …

In-situ Micromechanical Testing of Neutron Irradiated FeCrAl Alloys

Microstructure response of ferritic/martensitic steel HT9 after neutron irradiation: Effect of temperature

The ferritic/martensitic steel HT9 was irradiated in the BOR-60 reactor at 650, 690 and 730 K (377, 417 and 457 °C) to doses between ∼14.6–18.6 displacements per atom (dpa). Irradiated samples were comprehensively characterized using analytical …